Two-photon 3D printing diaphragm-integrated ring waveguide coupler for ultrasound detection.

We demonstrate a diaphragm-integrated ring waveguide coupler fabricated by the two-photon direct laser wring technique as an ultrasonic sensor, which is integrated on an optical fiber tip. The device consists of a micro-ring waveguide with a diameter of 5 µm functionalized as an optical fiber tip light reflection mirror and a straight waveguide connecting a diaphragm. The evanescent field coupling can be realized between the two waveguides, and the coupling efficiency can be changed due to the variation of the coupling gap induced by ultrasound. Accordingly, the light reflection can be changed. Based on the plate vibration theory, the vibration frequency can be changed through optimizing the diaphragm size. The experiments show that the device exhibits a high sensitivity and low noise equivalent acoustic signal level of 1.07 mPa/Hz1/2 at 100 kHz, which has great potential in various acoustic wave sensing applications.

Programmable Self-Regulation with Wrinkled Hydrogels and Plasmonic Nanoparticle Lattices.

This paper describes a self-regulating system that combines wrinkle-patterned hydrogels with plasmonic nanoparticle (NP) lattices. In the feedback loop, the wrinkle patterns flatten in response to moisture, which then allows light to reach the NP lattice on the bottom layer. Upon light absorption, the NP lattice produces a photothermal effect that dries the hydrogel, and the system then returns to the initial wrinkled configuration. The timescale of this regulatory cycle can be programmed by tuning the degree of photothermal heating by NP size and substrate material. Time-dependent finite element analysis reveals the thermal and mechanical mechanisms of wrinkle formation. This self-regulating system couples morphological, optical, and thermo-mechanical properties of different materials components and offers promising design principles for future smart systems.

Continuous tuning of unidirectional emission wavelength by bending a notched-elliptical polymer microdisk.

An approach of continuously tunable unidirectional emission through bending a notched-elliptical polymer microdisk is proposed. The characteristics of the bending-dependent action are carefully analyzed, and the resonance wavelength for unidirectional emission can be tuned continuously through bending the device. Such a whispering-gallery-mode microresonator enables unidirectional emission with ultra-low divergence, of which the emission efficiency and Q factor are stabilized, demonstrating the whole structure is robust and relatively insensitive within a certain bending angle range. A maximum resonance wavelength shift of ∼100 nm and Q factor of 1500 can be achieved with the total size of the microdisk less than 10 µm. This kind of microresonator is promising for applications in multilevel integrated photonics circuits and may open the door to new functionalities of resonator devices, from sensing to optical amplification.

Highly sensitive Mach-Zehnder interferometric micromagnetic field sensor based on 3D printing technology.

A two-photon 3D printed polymer magnetic sensing device based on a Mach-Zehnder interferometer (MZI) is proposed. One arm of the MZI contains a hollow cavity and two connecting open channels that can be filled with magnetic fluids (MFs) and sealed by the UV curable adhesive, forming a magneto-optical component of the interferometer. As the magnetic field changes, the refractive index (RI) of the MF changes, and the effective RI of the guiding mode of the waveguide changes accordingly, which results in a change in the phase of the MZI. The interferometric spectra can be used to evaluate the sensing sensitivity. The MZI structure with a hollow length of 40 µm is fabricated, and the microstructure is encapsulated with MF, demonstrating a highly sensitive magnetic field device. The experimental results show that the magnetic field sensitivity of the fabricated magnetic field device is -1.675nm/Oe. For a spectrometer with a resolution of 1 pm, the minimal detectable magnetic field resolution of the sensor is up to 59.7 nT with good stability.

Efficient harnessing of light from nanoscale emitters deterministically placed through polymer-pen lithography at the focus of 3D-printed ellipsoidal micro-lenses.

Collecting significant and measurable signals from the typically omnidirectional emission of nanoscale emitters is challenging. To improve the collection efficiency, it is essential to deterministically place the emitters in desired locations and design mode converters to match the modes of emission to those of the collection system. In this Letter, we propose the deterministic placement of nanoscale emitters using a pick-and-place technique called polymer-pen lithography. We demonstrate the concept with upconversion nanoparticles placed deterministically at the focus of three-dimensional-printed ellipsoidal micro-lenses. A significant part of the forward-going emission is collimated leading to increased collection efficiency, even at low numerical apertures of the collecting optics. The proposed approach lends itself to hybrid integration for fiber-to-chip and on-chip applications.

Large dynamic-range fiber Bragg grating sensor system for acoustic emission detection.

A distributed feedback (DFB) fiber laser and fiber Bragg gratings (FBGs) are configured to demodulate the wavelength shifts of FBG dynamic strain sensors. The FBG sensors act as sensing units to detect the dynamic strain and the demodulators while the DFB fiber laser only acts as a narrow-linewidth light source. As the reflective spectrum of the FBG sensor changes due to dynamic strains, the output is subsequently converted into a corresponding intensity change and detected directly by a photodetector. The 0.2 nm linewidth FBG sensor can detect the impact signal with a frequency of up to 300 kHz with a maximum of 29.17 µÉ›, which is comparable with the detecting result of the piezoelectric transducer sensor. Moreover, the directional response of the FBG sensor is maximized when the direction of acoustic wave propagation is parallel to the optical fiber. The relation between the sensitivity and the FBG spectrum linewidth is presented, and the detectable strain range versus different FBG linewidths is also discussed.

Inverse Design and 3D Printing of a Metalens on an Optical Fiber Tip for Direct Laser Lithography.

An inverse-designed metalens is proposed, designed, and fabricated on an optical fiber tip via a 3D direct laser-writing technique through two-photon polymerization. A computational inverse-design method based on an objective-first algorithm was used to design a thin circular grating-like structure to transform the parallel wavefront into a spherical wavefront at the near-infrared range. With a focal length about 8 µm at an operating wavelength of 980 nm and an optimized focal spot at the scale of 100 nm, our proposed metalens platform is suitable for two-photon direct laser lithography. We demonstrate the use of the fabricated metalens in a direct laser lithography system. The proposed platform, which combines the 3D printing technique and the computational inverse-design method, shows great promise for the fabrication and integration of multiscale and multiple photonic devices with complex functionalities.

Multi-wavelength microresonator based on notched-elliptical polymer microdisks with unidirectional emission.

A three-dimensional notched-elliptical microdisk with a wavelength-size notch on the boundary is proposed as a multi-wavelength and unidirectional emission lasing source. The device contains multiple properly designed two-dimensional whispering gallery mode-based polymer notched microdisks with different dimensions for use as a multi-wavelength source. It can have a relatively high optical quality factor of 4000, unidirectional emission with low far-field divergence ∼4°, and the efficiency of emission is as high as 84.2%. The effect of the notch size on the far-field divergence is analyzed, and the multi-wavelength lasing performance is characterized, demonstrating that the resonator is robust and reliable. This work paves a unique but generic way for the design of compact multi-wavelength microlasers.

Folding at the Microscale: Enabling Multifunctional 3D Origami-Architected Metamaterials.

Mechanical metamaterials inspired by the Japanese art of paper folding have gained considerable attention because of their potential to yield deployable and highly tunable assemblies. The inherent foldability of origami structures enlarges the material design space with remarkable properties such as auxeticity and high deformation recoverability and deployability, the latter being key in applications where spatial constraints are pivotal. This work integrates the results of the design, 3D direct laser writing fabrication, and in situ scanning electron microscopic mechanical characterization of microscale origami metamaterials, based on the multimodal assembly of Miura-Ori tubes. The origami-architected metamaterials, achieved by means of microfabrication, display remarkable mechanical properties: stiffness and Poisson's ratio tunable anisotropy, large degree of shape recoverability, multistability, and even reversible auxeticity whereby the metamaterial switches Poisson's ratio sign during deformation. The findings here reported underscore the scalable and multifunctional nature of origami designs, and pave the way toward harnessing the power of origami engineering at small scales.

Adaptive fiber-ring lasers based on an optical fiber Fabry-Perot cavity for high-frequency dynamic strain sensing.

A fiber-optic Fabry-Perot (FP) interferometer integrated with an adaptive fiber-ring laser is configured as a switchable multi-wavelength fiber laser that can be utilized for ultrasound detection. Because the FP sensor acts as a wavelength filter and a reflector of the fiber-ring laser, the reflective spectrum of the FP sensor changes due to static/dynamic strains, and the wavelength of the laser output shifts accordingly, which is subsequently converted into a corresponding phase shift and demodulated by an unbalanced interferometer. By carefully controlling the polarization of the system, the lasing outputs with a side-mode suppression ratio higher than 30 dB can be obtained, and the lasing linewidth is much narrower than that of the spectrum of the FP sensor. The experiments show that the proposed sensing system has high sensitivity for ultrasound detection and can be adaptive to the low-frequency drifts due to environmental noise.

Three-dimensional-printed Fabry-Perot interferometer on an optical fiber tip for a gas pressure sensor.

We demonstrate a three-dimensional (3D)-printed miniature optical fiber-based polymer Fabry-Perot (FP) interferometric pressure sensor based on direct femtosecond laser writing through two-photon polymerization. An unsealed cylinder column with a suspended polymer diaphragm is directly printed on a single-mode fiber tip to form an FP cavity. Here, two FP cavities with different lengths and the same diaphragm thickness (5 µm) are presented. The fabricated FP interferometer has a fringe contrast larger than 15 dB. The experimental results show that the fabricated device with a 140 µm cavity length has a linear response to the change of pressure with a sensitivity of 3.959 nm/MPa in a range of 0-1100 kPa, and the device with a 90 µm cavity length has a linear pressure sensitivity of 4.097 nm/MPa. The temperature sensitivity is measured to be about 160.2 pm/°C and 156.8 pm/°C, respectively, within the range from 20 to 70°C. The results demonstrate that 3D-printing techniques can be used for directly fabricating FP cavities on optical fiber tips for sensing applications.

Miniature resonator sensor based on a hybrid plasmonic nanoring.

A miniature resonator sensor based on a hybrid plasmonic nanoring with a gold layer coated uniformly on the outer boundary is described and investigated. By using the Lumerical finite-difference-time-domain (FDTD) method, the optimized sizes of the plasmonic layer thickness and the central hole are given and insight into the dependence of spectral displacements, Q factors, sensitivity and detection limits on the ambient refractive index is presented. Simulation results reveal that the miniature resonator sensor featuring high sensitivity of 339.8 nm/RIU can be realized. The highest Q factor can reach ∼60,000 with this nanoring and the minimum detection limit is as low as 1.5 × 10-4 RIU. The effects on the resonance shifts and Q factors due to geometric shapes of the inner boundary of the nanoring are discussed as well. This miniature resonator sensor has good potential for highly sensitive ultracompact sensing applications.

Direct laser writing of a phase-shifted Bragg grating waveguide for ultrasound detection.

We demonstrate a phase-shifted Bragg grating waveguide (PS-BGW) fabricated by a direct laser writing technique via two-photon polymerization as a high-frequency ultrasonic sensor. The PS-BGW device has a cross-sectional area of 1.5 µm×2 µm, and the grating length is about 100 µm. The optical resonant spectrum is investigated numerically and experimentally. The result shows that the fabricated device with a grating depth of 250 nm and a quarter wave phase lead to a 20-nm stopband and a 0.085-nm full-linewidth of the transmission notch, making it suitable for photonic sensing applications. Here, the PS-BGW device is demonstrated for the detection of acoustic waves, which can cause strain or deformation of the device and lead to a shift in the resonance wavelength. The sensitivity and the limitations of the device for ultrasound detection are also investigated.

Polymer micro-ring resonator integrated with a fiber ring laser for ultrasound detection.

Polymer micro-ring resonators fabricated by a direct laser writing technique are presented as sensors for ultrasound detection. The optical micro-ring resonator consists of a micro-ring waveguide that acts as a wavelength selective feedback mirror to an erbium-doped fiber-ring laser (FRL). The micro-ring resonator reflection spectrum determines the lasing frequencies of the FRL. Acoustic waves, which cause strain or deformation of the micro-ring resonator, lead to shifts of the resonance wavelength and thereby shifts in the FRL lasing spectrum. The spectral shifts are demodulated using an unbalanced Michelson interferometer. The experiments demonstrate that polymer micro-ring resonators integrated with a FRL can be used as adaptive high-frequency ultrasound detectors.

Comparative assessment of erbium fiber ring lasers and reflective SOA linear lasers for fiber Bragg grating dynamic strain sensing.

Fiber Bragg grating (FBG) dynamic strain sensors using both an erbium-based fiber ring laser configuration and a reflective semiconductor optical amplifier (RSOA)-based linear laser configuration are investigated theoretically and experimentally. Fiber laser models are first presented to analyze the output characteristics of both fiber laser configurations when the FBG sensor is subjected to dynamic strains at high frequencies. Due to differences in the transition times of erbium and the semiconductor (InP/InGaAsP), erbium-doped fiber amplifier (EDFA)- and RSOA-based fiber lasers exhibit different responses and regimes of stability when the FBG is subjected to dynamic strains. The responses of both systems are experimentally verified using an adaptive photorefractive two-wave mixing (TWM) spectral demodulation technique. The experimental results show that the RSOA-FBG fiber linear cavity laser is stable and can stably respond to dynamic strains at high frequencies. An example application using a multiplexed TWM interferometer to demodulate multiple FBG sensors is also discussed.

Fiber Bragg grating dynamic strain sensor using an adaptive reflective semiconductor optical amplifier source.

In this paper, a reflective semiconductor optical amplifier (RSOA) is configured to demodulate dynamic spectral shifts of a fiber Bragg grating (FBG) dynamic strain sensor. The FBG sensor and the RSOA source form an adaptive fiber cavity laser. As the reflective spectrum of the FBG sensor changes due to dynamic strains, the wavelength of the laser output shifts accordingly, which is subsequently converted into a corresponding phase shift and demodulated by an unbalanced Michelson interferometer. Due to the short transition time of the RSOA, the RSOA-FBG cavity can respond to dynamic strains at high frequencies extending to megahertz. A demodulator using a PID controller is used to compensate for low-frequency drifts induced by temperature and large quasi-static strains. As the sensitivity of the demodulator is a function of the optical path difference and the FBG spectral width, optimal parameters to obtain high sensitivity are presented. Multiplexing to demodulate multiple FBG sensors is also discussed.

Real-time full-field photoacoustic imaging using an ultrasonic camera.

A photoacoustic imaging system that incorporates a commercial ultrasonic camera for real-time imaging of two-dimensional (2-D) projection planes in tissue at video rate (30 Hz) is presented. The system uses a Q-switched frequency-doubled Nd:YAG pulsed laser for photoacoustic generation. The ultrasonic camera consists of a 2-D 12 x 12 mm CCD chip with 120 x 120 piezoelectric sensing elements used for detecting the photoacoustic pressure distribution radiated from the target. An ultrasonic lens system is placed in front of the chip to collect the incoming photoacoustic waves, providing the ability for focusing and imaging at different depths. Compared with other existing photoacoustic imaging techniques, the camera-based system is attractive because it is relatively inexpensive and compact, and it can be tailored for real-time clinical imaging applications. Experimental results detailing the real-time photoacoustic imaging of rubber strings and buried absorbing targets in chicken breast tissue are presented, and the spatial resolution of the system is quantified.

Bulk-wave and guided-wave photoacoustic evaluation of the mechanical properties of aluminum/silicon nitride double-layer thin films.

The development of devices made of micro- and nano-structured thin film materials has resulted in the need for advanced measurement techniques to characterize their mechanical properties. Photoacoustic techniques, which use pulsed laser irradiation to nondestructively induce very high frequency ultrasound in a test object via rapid thermal expansion, are suitable for nondestructive and non-contact evaluation of thin films. In this paper, we compare two photoacoustic techniques to characterize the mechanical parameters of edge-supported aluminum and silicon nitride double-layer thin films. The elastic properties and residual stresses in such films affect their mechanical performance. In a first set of experiments, a femtosecond transient pump-probe technique is used to investigate the Young's moduli of the aluminum and silicon nitride layers by launching ultra-high frequency bulk acoustic waves in the films. The measured transient signals are compared with simulated transient thermoelastic signals in multi-layer structures, and the elastic moduli are determined. Independent pump-probe tests on silicon substrate-supported region and unsupported region are in good agreement. In a second set of experiments, dispersion curves of the A(0) mode of the Lamb waves that propagate along the unsupported films are measured using a broadband photoacoustic guided-wave method. The residual stresses and flexural rigidities for the same set of double-layer membranes are determined from these dispersion curves. Comparisons of the results obtained by the two photoacoustic techniques are made and discussed.

Adaptive demodulation of dynamic signals from fiber Bragg gratings using two-wave mixing technology.

A two-wave mixing (TWM) interferometer using photorefractive (PRC) InP:Fe crystal is configured to demodulate the spectral shift of a fiber Bragg grating (FBG) sensor. The FBG is illuminated with a broadband source, and any strain in the FBG is encoded as a wavelength shift of the light reflected by the FBG. The wavelength shift is converted into phase shift by means of an unbalanced TWM interferometer. TWM wavelength demodulation is attractive for monitoring dynamic strains because it is adaptive and multiplexable. Adaptivity implies that it can selectively monitor dynamic strains without active compensation of large quasi-static strains and large temperature drifts that otherwise would cause system to drift. Multiplexability implies that several FBG sensors can be simultaneously demodulated using a single demodulator. TWM wavelength demodulation is therefore a cost-effective method of demodulating several spectrally encoded FBG sensors.

Interaction of a scanning laser-generated ultrasonic line source with a surface-breaking flaw.

The scanning laser source (SLS) technique has been proposed recently as an effective way to investigate small surface-breaking cracks. By monitoring the amplitude and frequency changes of the ultrasound generated as the SLS scans over a defect, the SLS technique has provided enhanced signal-to-noise performance compared to the traditional pitch-catch or pulse-echo ultrasonic methods. In previous work, either a point source or a short line source was used for generation of ultrasound. The resulting Rayleigh wave was typically bipolar in nature. In this paper, a scanning laser line source (SLLS) technique using a true thermoelastic line source (which leads to generation of monopolar surface waves) is demonstrated experimentally and through numerical simulation. Experiments are performed using a line-focused Nd:YAG laser and interferometric detection. For the numerical simulation, a hybrid model combining a mass-spring lattice method (MSLM) and a finite difference method (FDM) is used. As the SLLS is scanned over a surface-breaking flaw, it is shown both experimentally and numerically that the monopolar Rayleigh wave becomes bipolar, dramatically indicating the presence of the flaw.